Title of article :
Raman spectroscopy and TGA studies for the synthesis of multiwalled carbon nanotube-functionalized thiol (MWCNT-SH) nanocomposites: study of effect of concentration
Author/Authors :
Robati, D Islamshahr Branch - Islamic Azad University , Bagheriyan, S Shahryar Branch - Islamic Azad University , Rajabi, M Arak Branch - Islamic Azad University
Abstract :
We have investigated some methods such as
Raman spectroscopy and thermogravimetric analysis
(TGA) studies for the nanocomposites multi-walled carbon
nanotube-functionalized thiol (MWCNT-SH) by adding to
cysteamine with known concentration in nanocomposite.
For this study, we synthesized nanocomposite MWCNTSH by the reaction between multi-walled carbon nanotubes-functionalized carboxyl and the cysteamine. For
study of the effect of concentration, cysteamine with different concentrations was used (1, 3 and 5 % weight) and it
was called MWCNT-SH1, MWCNT-SH3 and MWCNTSH5, respectively. Then, the nanocomposite provided was
characterized by Fourier transform infrared spectroscopy
(FT-IR) and scanning electron microscope (SEM). The
surface structure of nanocomposites can be analyzed and
confirmed using Raman and FT-IR spectroscopy. Also, to
investigate the thermal stability TGA was used. The study
of TGA showed that nanocomposite MWCNT-SH had low
thermal stability at temperatures more than 100 C.
Keywords :
Raman spectroscopy , MWCNT , Functionalized thiol , Cysteamine , TGA
Journal title :
Astroparticle Physics