Title of article :
Synthesis and Characterization of Ferromagnetic CoBaO2.70 Nanoparticle with Ferromagnetic Properties
Author/Authors :
Akbarzadeh-T, N Department of Chemistry - University of Sistan and Baluchestan, Zahedan, Iran , Ramezanian-Ch, S Department of Chemistry - University of Sistan and Baluchestan, Zahedan, Iran
Pages :
9
From page :
108
To page :
116
Abstract :
In this research we report synthesis of a new Barium-Cobalt precursor complex with 2,6-pyridine dicarboxylic acid (dipic). The complex [Ba(H2O)6][Co(dipic)2] (1) has been characterized using spectral methods (FT-IR, UV-Vis), elemental analysis and Cyclic voltammetry (CV). We also report thermal decomposition of inorganic precursor complex (1). Characterization of the binary oxide nanoparticlewas carried out using Fourier Transform infrared (FT-IR) spectroscopy, X-ray powder diffraction (XRD), Scanning electron microscopy (SEM), Vibrating sample maghetometer (VSM) and energy dispersive X-ray analysis (EDX). The X-ray diffraction pattern at room temperature revealed that, highly pure and crystallized BaCoO2.70 in orthorhombic structure with a = 4.2300 Å, b = 4.3500 Å and c = 11.3200 Å.
Keywords :
Scanning electron microscopy , Cyclic voltammetry , X-ray diffraction
Journal title :
Inorganic Chemistry Research
Serial Year :
2019
Record number :
2513248
Link To Document :
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