Title of article :
Synthesis and Characterization of CoFe2O4 and CuFe2O4 Composited with Hematite by Impregnation Method to Remove Organic Pollutants
Author/Authors :
Gholami, Hedayat School of Metallurgy and Materials Engineering - University College of Engineering - University of Tehran - Tehran, Iran , Koohestani, Hassan Faculty of Material and Metallurgical Engineering - Semnan University - Semnan, Iran , Ahmadi, Mehdi Jam Petrochemical Company - Assaluyeh - Boushehr, Iran
Abstract :
In this research, using impregnation method, spinel cobalt and copper ferrites nanoparticles are
synthesized on the surface of hematite. Synthesized powders were characterized and examined by FTIR, XRF,
XRD, FESEM, BET and EDS analysis and the dye degradation was investigated by UV-vis and AAS methods.
Specific surface area increased especially in the sample containing cobalt, which indicates the precise of synthesis
and the creation of high surface nanoparticles at hematite surface. The size of particles was in the nano scale and
a good uniformity observed in the structure. The results indicated a significant increase in the catalytic ability of
hematite nanocomposite. Their catalytic capability investigated by the Fenton reaction with complete removal of
methylene blue from the solution via UV-vis irradiation. The samples stability discovered to be excellent by the
AAS method.
Keywords :
Fenton reaction , Spinel ferrites , Hematite/CoFe2O4 , Hematite/CuFe2O4 , Impregnation method
Journal title :
Iranian Journal of Materials Science and Engineering