Title of article :
The effect of MgCl2.6H2O and NaF on properties of Chitosan / HAAl 2O3 Scaffold
Author/Authors :
Mirjalili, Fatemeh Department of Material Engineering, Islamic Azad University Maybod Branch, Maybod , Kafashiyan, Ali Department of Material Engineering, Islamic Azad University Yazd Branch, Yazd , Salahi, Esmail Energy and Environmental Department - Materials and Energy Research Center, Karaj
Abstract :
The HA- Al2O3 nano composite was produced by precipitation method. In the
first study,
the effect of MgCl2.6H2O and NaF additives on HA-Al2O3 nano-composite powder
were studied and the second, chitosan / HA- Al2O3 scaffold was prepared by
freeze casting method. The phase and microstructure and morphology analysis
of nano composite and scaffold were performed by XRD, FT-IR, FESEM and TEM.
X-ray diffraction test results along with infrared spectroscopy indicated that, the
HA- Al2O3 nano composite without impurities were produced. TEM result showed
that, the produced nanocomposite particle sizes were reported between 30-50
nm.Moreover, the porosity percentages of scaffold without additive was about
56% and with NaF as an additive was about 63 %, however, the scaffold with
MgCl2.6H2O additive with 70% porosity had the highest porosity percentage. The
compressive strength of the SFA scaffold exhibited a two-fold strength compared
to the SMA scaffold, which indicated the improved mechanical compatibility of
the SFA scaffold.
Keywords :
Nano , Scaffold , HA , Alumina , Chitosan/ HA- Al2O3 , scaffold
Journal title :
Journal of Nanoanalysis