Title of article :
formation, characterization and thermal study of novel schiff base ligand from sulfonic acid and its complexes with co(ii), ni(ii), cu(ii), zn(ii) and hg(ii) type no
Author/Authors :
obaid, majida ibrahim university of baghdad - college of education for pure sciences (ibn al-haitham) - department of chemistry, iraq , jaafar, wurood ali university of baghdad - college of education for pure sciences (ibn al-haitham) - department of chemistry, iraq
Abstract :
the new liganed schiff base named [(e)-3-hydroxy-4-((3,4,5- trimethoxybenzylidene)amino) naphthalene-1- sulfonic acid] was synthesized from 3,4,5-trimethoxybenzyldehyde and 1-amino-2-aphthol-4- sulfonic acid in equal molar ratio. a series of new metal complexes of the common molecular formulation [m(l)2(h2o)2].h2o are synthesized and characterized by ir, uv–vis spectra, mass spectra, atomic absorption, elemental analyses, chloride content, magnetic susceptibility and conductivity measurements as well as thermo gravimetric analysis (tga, dsc). consistent with results of the magnetic and spectral studies, the advised geometrical structures for all of the prepared complexes have been octahedral formula.
Keywords :
azomethine , sulfonic acid , benzaldehyde
Journal title :
Chemical Methodologies
Journal title :
Chemical Methodologies