Author/Authors :
Xu, Xinyuan Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China , Wang, Chungui Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China , Zhou, Zhenghong Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China , Zeng, Zebing Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China , Ma, Xinpeng Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China , Zhao, Guofeng Nankai University - Institute of Elemento-Organic Chemistry, - State Key Laboratory of Elemento-Organic Chemistry, China , Tang, Chuchi Nankai University - Institute of Elemento-Organic Chemistry - State Key Laboratory of Elemento-Organic Chemistry, China
Abstract :
Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in theformation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity( 95%, determined by 1H NMR and elemental analyses).
Keywords :
N , Thiophosphoryl imine , thermal condensation , thiophosphoramide , acetal
