Title of article
A convenient gram-scale synthesis of uridine diphospho(13C6)glucose
Author/Authors
Zoran Dinev، نويسنده , , Ahmad Z. Wardak، نويسنده , , Robert T.C Brownlee، نويسنده , , Spencer J. Williams، نويسنده ,
Issue Information
دوهفته نامه با شماره پیاپی سال 2006
Pages
5
From page
1743
To page
1747
Abstract
A simple gram-scale synthesis of uridine diphospho(13C6)glucose is presented from d-(13C6)glucose. The critical step uses a 1H-tetrazole-catalyzed coupling of 2,3,4,6-tetra-O-acetyl-α-d-glucopyranosyl-1-phosphate and UMP-morpholidate. The uridine diphospho(13C6)glucose was used in the structural identification of (1→3)-β-d-glucan from Lolium multiflorum.
Keywords
Morpholidate coupling , Isotopic labeling , Glucan , UDP-glucose , Sugar nucleotides
Journal title
Carbohydrate Research
Serial Year
2006
Journal title
Carbohydrate Research
Record number
965795
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