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New 12-Tungstophosphate-Based Organic-Inorganic Hybrid. Synthesis, Spectroscopic Characterization, X-Ray Determination and Thermal Behavior

Pourayoubi M. نويسنده , Mahjoub A.R. نويسنده , Maleki F. نويسنده , Ghammamy S. نويسنده , Lavaee P. نويسنده

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12-Tungstophosphate-based organic/inorganic hybrid, [HNMPA]3[O40PW12].0.5NMPA.2H2O (NMPA = N-methylpropionamide) was synthesized and characterized by IR, UV-Vis, 1H, 13C and 31P NMR spectroscopies, elemental analysis, TGA, DTA and single crystal X-ray determination. Full decomposition of the hybrid leads to WO3 powder was studied by IR, SEM and XRD.

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