شماره ركورد :
33227
عنوان مقاله :
Synthesis and Characterization of newthiadiazol and pyrimidine Derivatives
پديد آورندگان :
hays, qusay . h. basrah university - education college for pure science - chem. dept., Basrah, Iraq , shihabaldain, nezar. l. basrah university - education college for pure science - chem. dept., Basrah, Iraq
از صفحه :
320
تا صفحه :
336
چكيده فارسي :
This Study include the synthesis of Five and Six membered ring hetero cyclic compounds ,and we can be divided the work by two parts. Part one Includes Synthesis 2-amino -5-mercapto -1,3,4- thiadiazol(AMT)and then preparedifferent Schiff basewhich is prepared from AMT reacted with different Subsitauted aldehydes.Part twoIncludes preparation new pyrimidine derivative . Preparation the pyrimidine derivatives was through reacting two different types of chalcone with Urea presence 5ml of concentrated hydrochloric acidwhich are then neutralized with ammonium hydroxide. All compounds are identified by (FT:IR), and Mass and C 13-NMR and Some compounds by H1-NMR
كليدواژه :
1 , 3 , 4 , thiadiazol , pyrimidine
عنوان نشريه :
ابحاث ميسان
لينک به اين مدرک :
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