شماره ركورد كنفرانس :
4518
عنوان مقاله :
Synthesis of sulfated zirconia nanopowders for catalytic applications
Author/Authors :
M Ejtemaei Chemical Engineering Department - Sahand University of Technology , A Tavakoli Chemical Engineering Department - Sahand University of Technology , A.A Babaluo Chemical Engineering Department - Sahand University of Technology , B Bayati Chemical Engineering Department - Sahand University of Technology , N Charchi Chemical Engineering Department - Sahand University of Technology
كليدواژه :
Sulfated zirconia , Polyacrylamide gel , Calcination temperature , Sulfate ion
عنوان كنفرانس :
The 7th International Chemical Engineering Congress & Exhibition (IChEC 2011
چكيده لاتين :
Synthesis of sulfated zirconia nanopowders using the polyacrylamide gel method was carried out.
An assessment of the influence of the calcinations temperature (500-650 C) and sulfate ion (SO4
2-)
loading on the properties of SO4
2--ZrO2 was performed and characterized using X-ray diffraction
(XRD), spectroscopy electron microscopy (SEM) techniques.FTIR analysis was used to confirm
the presence of sulfate groups. Our experimental results showed that tetragonal phase crystalline
structure appeared for all the catalysts calcined at 500–650 C and also proprties of sulfated
zirconia is affected by amount of sulfate ion loading.