DocumentCode :
1059785
Title :
Interpretation of X-Ray Line Profile of Polycrystalline {\\hbox {MgB}}_{2}
Author :
Hanafusa, Kei ; Yamamoto, Akiyasu ; Ogino, Hiraku ; Horii, Shigeru ; Shimoyama, Jun-ichi ; Kishio, Kohji
Author_Institution :
Dept. of Appl. Chem., Univ. of Tokyo, Tokyo, Japan
Volume :
19
Issue :
3
fYear :
2009
fDate :
6/1/2009 12:00:00 AM
Firstpage :
2690
Lastpage :
2693
Abstract :
XRD peak profile analysis was performed on polycrystalline MgB2 bulks and tapes manufactured by various heat treatment conditions in order to investigate statistical value of crystallite size. Volume-weighted and area-weighted mean diameter of a bulk sample heated at 600degC for 6 h were estimated to be approximately 90 nm and 20 nm, respectively. These suggest that crystallite size distribution of MgB2 is very wide, although a lot of very small crystallites exist. Similar tendencies were observed for other samples. On the other hand J c values were found to be rather low compared to the expected values considering its small D a . This indicates that a small portion of crystallite interfaces act as effective pinning centers.
Keywords :
X-ray diffraction; critical current density (superconductivity); crystallites; flux pinning; grain size; heat treatment; magnesium compounds; sintering; superconducting critical field; superconducting materials; superconducting tapes; MgB2; X-ray line profile; area-weighted mean diameter; critical current density; crystallite size; flux pinning force; grain size; heat treatment; mono-core superconducting tapes; pinning centers; polycrystalline superconducting materials; powder-in-closed-tube method; sintering; temperature 600 C; time 6 h; upper critical field; volume-weighted mean diameter; Crystallite size; X-ray line profile analysis; magnesium diboride; polycrystalline bulks and tapes;
fLanguage :
English
Journal_Title :
Applied Superconductivity, IEEE Transactions on
Publisher :
ieee
ISSN :
1051-8223
Type :
jour
DOI :
10.1109/TASC.2009.2018116
Filename :
5067108
Link To Document :
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