Title :
Improvement of IBAD MgO template layers on metallic substrates for YBCO HTS deposition
Author :
Groves, J.R. ; Arendt, P.N. ; Foltyn, S.R. ; Jia, Q.X. ; Holesinger, T.G. ; Emmert, L.A. ; DePaula, R.F. ; Dowden, P.C. ; Stan, L.
Author_Institution :
Supercond. Technol. Center, Los Alamos, NM, USA
fDate :
6/1/2003 12:00:00 AM
Abstract :
We present our results to improve ion beam assisted deposition (IBAD) of magnesia (MgO) templates for subsequent YBa2Cu3O7-δ (YBCO) deposition. The substrate surface roughness has a significant effect on the initial nucleation texture of IBAD MgO films. We have found that reduction in our substrate surface roughness to ∼ 3.5 nm has resulted in better in-plane texture for IBAD MgO films than those deposited on rougher metal substrates. We have further improved the IBAD MgO deposition parameters by using an in situ reflected high-energy electron diffraction (RHEED) analysis tool that allows for monitoring of IBAD MgO growth. We have found a direct correlation between the RHEED generated intensity versus time curve and in-plane texture. Utilizing X-ray diffraction analysis, we have been able to determine the optimum deposition parameters to routinely grow films in batch mode that have a phi scan Δφ from 6 - 7°. Coupling the improvements in substrate preparation with optimization of IBAD MgO deposition has allowed for both batch and continuous deposition (termed c-IBAD MgO) on metallic substrates that result in superior superconducting properties. We have demonstrated that deposited meter lengths have had phi scan FWHM values from 8 - 9° with ± 10% uniformity. Additionally, we have been able to widen the processing zone in our system and coat two, one-meter lengths simultaneously while preserving good texture quality (Δφave ∼ 8°) and uniformity (60 - 80% of tape length within ± 5% of Δφave) for both tapes.
Keywords :
X-ray diffraction; barium compounds; high-temperature superconductors; ion beam assisted deposition; magnesium compounds; nucleation; reflection high energy electron diffraction; superconducting thin films; texture; yttrium compounds; MgO; RHEED; X-ray diffraction; YBCO HTS thin film; YBa2Cu3O7; ion beam assisted deposition; magnesia template; metallic substrate; nucleation texture; superconducting properties; surface roughness; High temperature superconductors; Ion beams; Magnesium compounds; Optical films; Rough surfaces; Superconducting films; Surface roughness; Surface texture; X-ray diffraction; Yttrium barium copper oxide;
Journal_Title :
Applied Superconductivity, IEEE Transactions on
DOI :
10.1109/TASC.2003.811937