Title :
K2Mo4O13 nanobelts: synthesis and properties
Author :
Zhiyi Zhang ; Chenguo Hu ; Yabo Zhu ; Shoudong Xu ; Xiaoshan He ; Hashim, Mazlan ; Donghu Xiang
Author_Institution :
Dept. of Appl. Phys., Chongqing Univ., Chongqing, China
fDate :
8/1/2011 12:00:00 AM
Abstract :
This Letter describes a simple molten salt approach to the synthesis of K2Mo4O13 nanobelts with lengths of several tens of micrometres. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction spectrum and energy dispersive spectroscopy are used to characterise the structure, morphology and composition of the sample. The UV-visible spectrum shows that the bandgap of the K2Mo4O13 nanobelts is 3.6 eV. Photoluminescence measurement shows a strong and broad emission peak of 355 nm for the K2Mo4O13 nanobelts. Electrochemical tests show good performance of the material in cycling stability as cathode material for Li-ion batteries.
Keywords :
X-ray chemical analysis; X-ray diffraction; cathodes; electrochemical analysis; electrochemical electrodes; energy gap; nanofabrication; nanostructured materials; photoluminescence; potassium compounds; scanning electron microscopy; secondary cells; transmission electron microscopy; ultraviolet spectra; visible spectra; EDS; K2Mo4O13; Li-ion batteries; SEM; TEM; UV-visible spectrum; X-ray diffraction spectrum; XRD; bandgap; cathode material; cycling stability; electrochemical tests; emission peak; energy dispersive spectroscopy; nanobelts; photoluminescence measurement; scanning electron microscopy; simple molten salt approach; transmission electron microscopy; wavelength 355 nm;
Journal_Title :
Micro & Nano Letters, IET
DOI :
10.1049/mnl.2011.0355