Influence of synthesis temperature on synthesis of PVA-stabilised silver nanoparticles

Author

Siva Kumar, K. ; Divya, A. ; Pavan Kumar, S. ; Ajitha, B. ; Chaithanya, V.S. ; Jaya Prasad, K. ; Sreedhara Reddy, P.

Author_Institution

Dept. of Phys., Sri Venkateswara Univ., Tirupati, India

Volume

6

Issue

11

fYear

2011

Firstpage

975

Lastpage

977

Abstract

Polyvinyl alcohol (PVA)-stabilised silver nanoparticles have been synthesised by the simple reduction process at different temperatures ranging from 60 to 90°C. The as-synthesised silver nanoparticles were analysed by X-ray diffraction (XRD), energy-dispersive analysis of X-rays, transmission electron microscope, UV°vis absorption spectroscopy and Fourier transform infrared (FTIR) spectroscopy. XRD studies showed that the samples exhibited cubic structure. The average particle size was found to be °50°nm. FTIR spectra revealed that the synthesised nanoparticles were successively capped by PVA. Optical absorption spectra confirmed the uniformity of as-prepared silver nanoparticles and the absorption peak was observed in the range 390°421°nm.

Keywords

Fourier transform spectra; X-ray chemical analysis; X-ray diffraction; infrared spectra; nanofabrication; nanoparticles; particle size; polymers; silver; transmission electron microscopy; ultraviolet spectra; visible spectra; Ag; FTIR; Fourier transform infrared spectroscopy; UV-vis absorption spectroscopy; X-ray diffraction; XRD; cubic structure; energy-dispersive X-ray analysis; optical absorption spectra; particle size; polyvinyl alcohol-stabilised silver nanoparticles; temperature 60 degC to 90 degC; transmission electron microscopy;

fLanguage

English

Journal_Title

Micro & Nano Letters, IET

Publisher

iet

ISSN

1750-0443

Type

jour

DOI

10.1049/mnl.2011.0516

Filename

6096517