Title :
Formation of porous and dense Pt/C catalyst films using electrohydrodynamic atomisation deposition
Author :
Dazhi Wang ; Hongbin Duan ; Junsheng Liang ; Chong Liu
Author_Institution :
Key Lab. for Micro/Nano Technol. & Syst. of Liaoning Province, Dalian Univ. of Technol., Dalian, China
fDate :
3/1/2012 12:00:00 AM
Abstract :
In this Letter, electrohydrodynamic atomisation (EHDA) was used to spray deposit Pt/C catalyst films using a Pt/C nanosuspension. In stable cone-jet atomisation mode, the influence of flow rate on the characteristics of relics and films was analysed. At a lower flow rate smaller size and lower number density of relics were predominant, which led to the formation of porous films; conversely, higher flow rate generated dense films. The size of the relics in experimental results and theoretically predicted size were compared and analysed. The dispersive X-ray analysis confirms that the EHDA deposited films are Pt/C.
Keywords :
X-ray chemical analysis; carbon; catalysts; electrohydrodynamics; nanofabrication; nanoporous materials; platinum; porous materials; spraying; suspensions; thin films; EHDA deposited films; Pt-C; catalyst films; dispersive X-ray analysis; electrohydrodynamic atomisation deposition; flow rate; nanosuspension; porous films; stable cone-jet atomisation mode;
Journal_Title :
Micro & Nano Letters, IET
DOI :
10.1049/mnl.2012.0018