DocumentCode :
1522221
Title :
Gold/hydroxypropyl cellulose hybrid nanocomposite constructed with more complete coverage of gold nano-shell
Author :
Sadeghi, B. ; Ghammamy, S. ; Gholipour, Z. ; Ghorchibeigy, M. ; Nia, A Amini
Author_Institution :
Dept. of Chem., I.A.U., Tonekabon, Iran
Volume :
6
Issue :
4
fYear :
2011
fDate :
4/1/2011 12:00:00 AM
Firstpage :
209
Lastpage :
213
Abstract :
The gold nanocomposite supported on hydroxypropyl cellulose (HPC) using NaBH4 as a medium has been prepared successfully here. A brownish-red solution in its UV-vis absorption spectrum showed surface plasmon resonance absorption bands between 520 and 560-nm in solutions. The Au/HPC nanocomposite was characterised by X-ray diffraction (XRD) measurement, transmission electron microscopy (TEM), scanning electron microscopy (SEM) and thermogravimetric analysis (TGA). XRD showed the fcc crystal structure of the bulk Au with particles of less than 22-nm in size similar to that is observed by TEM and HPC is crucial for the formation of such gold nanocomposite. SEM indicated uniform distribution of particles in the film. TGA confirmed enhanced thermal stability of the polymer. This easy synthetic approach to gold nano- and microstructures is a seedless, one-step, fast, template-free route that shows good reproducibility and may be further developed to produce other types of metal nanostructures that satisfy specific applications.
Keywords :
X-ray diffraction; crystal structure; filled polymers; gold; nanocomposites; nanofabrication; organic-inorganic hybrid materials; scanning electron microscopy; surface plasmon resonance; thermal analysis; thermal stability; transmission electron microscopy; ultraviolet spectra; visible spectra; Au; SEM; TEM; TGA; UV-vis absorption spectrum; X-ray diffraction; XRD; brownish-red solution; crystal structure; gold nanoshell; gold-hydroxypropyl cellulose hybrid nanocomposite; polymer; scanning electron microscopy; surface plasmon resonance absorption bands; thermal stability; thermogravimetric analysis; transmission electron microscopy; wavelength 520 nm to 560 nm;
fLanguage :
English
Journal_Title :
Micro & Nano Letters, IET
Publisher :
iet
ISSN :
1750-0443
Type :
jour
DOI :
10.1049/mnl.2011.0036
Filename :
5771625
Link To Document :
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