• DocumentCode
    1522221
  • Title

    Gold/hydroxypropyl cellulose hybrid nanocomposite constructed with more complete coverage of gold nano-shell

  • Author

    Sadeghi, B. ; Ghammamy, S. ; Gholipour, Z. ; Ghorchibeigy, M. ; Nia, A Amini

  • Author_Institution
    Dept. of Chem., I.A.U., Tonekabon, Iran
  • Volume
    6
  • Issue
    4
  • fYear
    2011
  • fDate
    4/1/2011 12:00:00 AM
  • Firstpage
    209
  • Lastpage
    213
  • Abstract
    The gold nanocomposite supported on hydroxypropyl cellulose (HPC) using NaBH4 as a medium has been prepared successfully here. A brownish-red solution in its UV-vis absorption spectrum showed surface plasmon resonance absorption bands between 520 and 560-nm in solutions. The Au/HPC nanocomposite was characterised by X-ray diffraction (XRD) measurement, transmission electron microscopy (TEM), scanning electron microscopy (SEM) and thermogravimetric analysis (TGA). XRD showed the fcc crystal structure of the bulk Au with particles of less than 22-nm in size similar to that is observed by TEM and HPC is crucial for the formation of such gold nanocomposite. SEM indicated uniform distribution of particles in the film. TGA confirmed enhanced thermal stability of the polymer. This easy synthetic approach to gold nano- and microstructures is a seedless, one-step, fast, template-free route that shows good reproducibility and may be further developed to produce other types of metal nanostructures that satisfy specific applications.
  • Keywords
    X-ray diffraction; crystal structure; filled polymers; gold; nanocomposites; nanofabrication; organic-inorganic hybrid materials; scanning electron microscopy; surface plasmon resonance; thermal analysis; thermal stability; transmission electron microscopy; ultraviolet spectra; visible spectra; Au; SEM; TEM; TGA; UV-vis absorption spectrum; X-ray diffraction; XRD; brownish-red solution; crystal structure; gold nanoshell; gold-hydroxypropyl cellulose hybrid nanocomposite; polymer; scanning electron microscopy; surface plasmon resonance absorption bands; thermal stability; thermogravimetric analysis; transmission electron microscopy; wavelength 520 nm to 560 nm;
  • fLanguage
    English
  • Journal_Title
    Micro & Nano Letters, IET
  • Publisher
    iet
  • ISSN
    1750-0443
  • Type

    jour

  • DOI
    10.1049/mnl.2011.0036
  • Filename
    5771625