Synthesis and structural characterization of nickel oxide nanoparticles synthesized by Polymerized complexed (PC) method

Author

Wongsaprom, K. ; Maensiri, S.

Author_Institution

Dept. of Phys., Mahasarakham Univ., Mahasarakham, Thailand

fYear

2010

Firstpage

1044

Lastpage

1045

Abstract

Nickel oxide (NiO) nanoparticles with particle size around 30-40 nm have been synthesized via polymerized complex method. In this method, citric acid was used as a reagent and ethylene glycol was used as a polymer stabilizer and also served as a diffusion barrier. The synthesized precursors were calcined at 773, 873 and 973 K for 4 h to obtain the nickel oxide nanoparticles. The structure, morphology, crystalline phase and particle sizes were investigated by XRD, SEM, TEM, UV-vis and FT-IR.

Keywords

Fourier transform spectra; X-ray diffraction; calcination; crystal morphology; infrared spectra; nanofabrication; nanoparticles; nickel compounds; particle size; scanning electron microscopy; transmission electron microscopy; ultraviolet spectra; visible spectra; FTIR spectra; NiO; SEM; TEM; UV-vis spectra; XRD; calcination; citric acid; crystalline phase; diffusion barrier; ethylene glycol; morphology; nanoparticle synthesis; particle size; polymer stabilizer; polymerized complexed method; structural characterization; temperature 773 K to 973 K; Crystallization; Equations; Magnetic materials; Morphology; Nanoparticles; Nickel; Numerical analysis; Physics; Polymers; X-ray scattering;

fLanguage

English

Publisher

ieee

Conference_Titel

Nanoelectronics Conference (INEC), 2010 3rd International

Conference_Location

Hong Kong

Print_ISBN

978-1-4244-3543-2

Electronic_ISBN

978-1-4244-3544-9

Type

conf

DOI

10.1109/INEC.2010.5425049

Filename

5425049