Title :
Microfabricated preconcentrator for quantitative analysis of low concentration volatile organic compounds
Author :
Chan, Helena K L ; Pang, Stella W. ; Veeneman, Rebecca A. ; Zellers, Edward T. ; Takei, Masahiko
Author_Institution :
Eng. Res. Center for Wireless Integrated Microsystems, Michigan Univ., Ann Arbor, MI, USA
Abstract :
A microfabricated preconcentrator that demonstrates vapor trapping ability for part-per-billion volatile organic compounds and integrated temperature sensing for heat transfer measurements is demonstrated. The preconcentrator design accommodates 3.3 mg of carbon adsorbents in a series of three 450 m deep Si cavities fabricated using deep reactive ion etching and sealed using wafer-level Au-Au thermocompression bonding at 400 °C. Backside Pt resistance temperature detectors (RTDs) are integrated to monitor heating rates and study forced convective heat transfer during the thermal desorption cycle where the preconcentrator is heated to 300 °C. The preconcentrator is being developed to enable high-speed chromatographic separations as a part of a low-power, portable microscale gas chromatography system.
Keywords :
chromatography; heat transfer; lead bonding; micromachining; organic compounds; sputter etching; temperature sensors; 3.3 mg; 300 C; 400 C; carbon adsorbents; chromatographic separations; deep reactive ion etching; forced convective heat transfer; gas chromatography; heat transfer measurements; microfabricated preconcentrator; quantitative analysis; resistance temperature detectors; temperature sensor; thermal desorption cycle; thermocompression bonding; vapor trapping ability; volatile organic compounds; Detectors; Electrical resistance measurement; Etching; Heat transfer; Monitoring; Resistance heating; Temperature sensors; Thermal resistance; Volatile organic compounds; Wafer bonding;
Conference_Titel :
Solid-State Sensors, Actuators and Microsystems, 2005. Digest of Technical Papers. TRANSDUCERS '05. The 13th International Conference on
Print_ISBN :
0-7803-8994-8
DOI :
10.1109/SENSOR.2005.1497515