Title :
Liquid Phase Electrochemical Route to Carbon Nanotubes at Room Temperature
Author :
Cheng, H.S. ; Shen, M.R. ; Mak, C.L. ; Lim, P.K.
Author_Institution :
Dept. of Phys., Hong Kong Baptist Univ., Kowloon
Abstract :
A novel room temperature synthesis of carbon nanotubes (CNTs) by liquid phase deposition of methanol is firstly reported. Nanotube samples were characterized with field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and Raman spectroscopy. FESEM micrographs revealed that nanotubes with diameter in the range of 20-200 nm were grown at room temperature. HR-TEM images and electron diffraction pattern demonstrated that the as-grown nanotubes were multi-wall carbon nanotubes (MWCNTs). Furthermore, Raman spectra of the nanotubes showed two strong characteristic vibrational modes at 1352 cm-1 and 1585 cm-1, Raman peaks commonly found for carbon nanotubes
Keywords :
Raman spectra; carbon nanotubes; electrochemistry; electron diffraction; field emission electron microscopy; liquid phase deposition; scanning electron microscopy; transmission electron microscopy; vibrational modes; 20 to 200 nm; 293 to 298 K; C; CNT Raman peaks; CNT vibrational modes; FESEM; MWCNT; Raman spectroscopy; TEM; electron diffraction; field emission scanning electron microscopy; liquid phase electrochemical synthesis method; methanol liquid phase deposition; multi-wall carbon nanotubes; room temperature CNT synthesis; transmission electron microscopy; Carbon nanotubes; Costs; Electron emission; Fabrication; Methanol; Micromechanical devices; Physics; Polarization; Substrates; Temperature; Carbon nanotube; RTM; component; electrodeposition; methanol;
Conference_Titel :
Nano/Micro Engineered and Molecular Systems, 2006. NEMS '06. 1st IEEE International Conference on
Conference_Location :
Zhuhai
Print_ISBN :
1-4244-0139-9
Electronic_ISBN :
1-4244-0140-2
DOI :
10.1109/NEMS.2006.334823