Title :
The use of microwave energy for obtaining dry silica sol
Author :
Bortishevsky, V.A. ; Kashkovsky, V.I. ; Novikova, I.A. ; Zagorodny, V.V. ; Launets, V.L. ; Oliynik, V.V.
Author_Institution :
Inst. for Bioorg. Chem. & Petrochem., Kyiv, Ukraine
Abstract :
Presented in this work is an original technique of obtaining high-concentration silica sols which are widely used in various branches of industry. This technique consists of three stages: synthesis, stabilization and drying of the silica sols. Microwave evaporation was used at the stage of final drying and removed the local hot spots of the drying substance, thus helping to avoid the formation of a non-reversible gel. The silica sol was dehydrated till 60% concentration and then placed in the chamber of a teflon reactor. The experiment was carried out at one of the industrial frequencies. The uninterrupted mode of generation was used. Silica sol obtained in this way is 100% reversible, e.g. its dry powder disperses in water to a 100% extent, forming an initial colloidal solution.
Keywords :
drying; evaporation; materials preparation; microwave heating; silicon compounds; sols; SiO/sub 2/; dehydration; dry silica sol; drying; high-concentration silica sols; microwave energy; microwave evaporation; stabilization; synthesis; teflon reactor; uninterrupted generation mode; Bills of materials; Chromium; Helium; Indium tin oxide; Microwave technology; Organizing; Silicon compounds;
Conference_Titel :
Microwave Conference, 2000. Microwave and Telecommunication Technology. 2000 10th International Crimean
Conference_Location :
Crimea, Ukraine
Print_ISBN :
966-572-048-1
DOI :
10.1109/CRMICO.2000.1256231