Title :
Formation of α-MoO3 (010) micropalettes for nanoarchitecture
Author :
Troitskaia, Irina B. ; Atuchin, Viktor V. ; Gavrilova, Tatiana A. ; Sheglov, Dmitriy V.
Author_Institution :
Lab. of Opt. Mater. & Struct., SB RAS, Novosibirsk, Russia
fDate :
June 30 2011-July 4 2011
Abstract :
α-MoO3 micropalettes with high-quality surface have been formed by annealing of intermediate molybdenum oxide at T = 650°C in air. The intermediate molybdenum oxide was prepared by thermal decomposition of molybdenum formate at T = 450°C under oxygen deficiency. The chemical composition, structure and micromorphology of intermediate products and α-MoO3 micropalettes have been examined with XRD, SEM, AFM, TG/DSC and IR spectroscopy. The results indicate the formation of α-MoO3 micropalettes with ~50 μm length, ~10 μm width and ~600 nm thickness, developed (010) crystal plane and high-quality flat surface.
Keywords :
X-ray diffraction; annealing; atomic force microscopy; crystal growth; differential scanning calorimetry; infrared spectroscopy; molybdenum compounds; precipitation (physical chemistry); scanning electron microscopy; AFM; IR spectroscopy; MoO3; SEM; TG/DSC; XRD; annealing; crystal plane; high-quality flat surface; micropalettes; nanoarchitecture; oxygen deficiency; temperature 450 degC; temperature 650 degC; thermal decomposition; Chemicals; Crystals; Optical films; Optical surface waves; Substrates; X-ray scattering; Molybdenum oxide; microcrystal; precipitation; structure;
Conference_Titel :
Micro/Nanotechnologies and Electron Devices (EDM), 2011 International Conference and Seminar of Young Specialists on
Conference_Location :
Erlagol, Altai
Print_ISBN :
978-1-61284-793-1
DOI :
10.1109/EDM.2011.6006882
