Title :
Nanostructure sensor films preparation by extraction-pyrolysis technique
Author :
Patrusheva, T.N.
Author_Institution :
Polytech. Inst. of Siberian Fed. Univ., Krasnoyarsk
Abstract :
We propose the extraction-pyrolysis technique for deposition of nanostructure films of oxide functional materials. The carboxylic acids have been used as extragent. The extraction process was realized by cation exchange mechanism. At the selective extraction the anions of inorganic salts and impurities of cations was not extracted in organic phase. Therefore, the application of extraction allows obtaining pure materials. In order to adjusting of metals concentration the extracts undergoes to analysis by atomic absorption spectroscopy. To determination the decomposition temperature TG-LTA investigations have been carried out. It was found that thermal decomposition of metal-carboxylates take place at 400 - 450 degC.
Keywords :
atomic absorption spectroscopy; microsensors; nanotechnology; pyrolysis; TG-LTA; atomic absorption spectroscopy; carboxylic acids; cation exchange mechanism; decomposition temperature; extraction-pyrolysis technique; nanostructure sensor films preparation; oxide functional materials; pure materials; selective extraction; thermal decomposition; Conducting materials; Conductive films; Conductivity; Gases; Microstructure; Nanostructured materials; Optical films; Solids; Substrates; Temperature sensors; composite oxides; extraction; homogeneity; nanosize materials; purity; solution technology;
Conference_Titel :
Physics of Semiconductor Devices, 2007. IWPSD 2007. International Workshop on
Conference_Location :
Mumbai
Print_ISBN :
978-1-4244-1728-5
Electronic_ISBN :
978-1-4244-1728-5
DOI :
10.1109/IWPSD.2007.4472675