Title :
In-situ transmission electron microscopy studies on the dynamic behaviors of materials
Author :
Mori, Hirotaro ; Arakawa, Kazuto ; Lee, Jung Goo ; Chen, Chun Lin
Author_Institution :
Res. Center for Ultrahigh-Voltage Electron Microscopy, Osaka Univ., Ibaraki, Japan
Abstract :
Topics of in-situ transmission electron microscopy studies on the dynamic behaviors of materials are described. Estimation of the activation energy for the migration of self-interstitial atoms is successfully carried out. The coalescence between nm-scale prismatic dislocation loops with different Burgers vectors, as well as the one-dimensional glide diffusion of the loops, has been confirmed. A new electron-beam-induced deposition method using no precursor gas, has been developed for the fabrication of tungsten nanostructures. Size dependence of the eutectic temperature of alloy particles was examined. A linear relationship between the eutectic temperature and the inverse radius of the particle was obtained. In-situ experiments with TEM are useful in revealing the dynamic behaviors of materials.
Keywords :
diffusion; dislocation loops; electron beam deposition; eutectic alloys; interstitials; lead alloys; nanofabrication; nanoparticles; silver alloys; transmission electron microscopy; tungsten; AgPb; Burgers vectors; W; activation energy; alloy particles; coalescence; dynamic properties; electron-beam-induced deposition method; eutectic temperature; in-situ transmission electron microscopy; inverse particle radius; one-dimensional glide diffusion; prismatic dislocation loops; self-interstitial atoms; size dependence; tungsten nanostructures; Atomic measurements; Estimation; Fabrication; Materials; Metals; Microstructure; Nanostructures;
Conference_Titel :
Nanotechnology Materials and Devices Conference (NMDC), 2011 IEEE
Conference_Location :
Jeju
Print_ISBN :
978-1-4577-2139-7
DOI :
10.1109/NMDC.2011.6155317