Title :
Synthesis and characterization of TbMnO3 nanorods
Author :
Sinha, S. ; Mukherjee, A. ; Chatterjee, S.K. ; Meikap, A.K. ; Basu, S.
Author_Institution :
Dept. of Phys., Nat. Inst. of Technol., Durgapur, India
Abstract :
We report the synthesis and characterization of multiferroic TbMnO3 nanorods by sol-gel route. From XRD analysis it was observed that annealing at 700°C for 2h is the most favorable condition for the fabrication of TbMnO3 nano rods. The TEM study revealed that the diameter of these rods varied from 12.6 38.1 nm and the length of these nanorods varied from 88.6-292 nm. SAED pattern of the nano rods revealed single crystalline structure. Presence of TbMnO3 nano particles was also observed along with the nanorods. UV,PL, F.T.I.R study on the samples annealed at different calcination condition is also reported.
Keywords :
Fourier transform spectra; X-ray diffraction; annealing; calcination; infrared spectra; multiferroics; nanofabrication; nanorods; photoluminescence; sol-gel processing; terbium compounds; transmission electron microscopy; ultraviolet spectra; FTIR; PL spectroscopy; SAED pattern; TEM; TbMnO3; UV spectroscopy; XRD analysis; annealing; calcination; multiferroic nanorods; nanoparticles; single crystalline structure; sol-gel route; temperature 700 degC; time 2 h; Annealing; Heating; Magnetic resonance imaging; Optical coupling; Optical imaging; Optical polarization; X-ray scattering; HR-TEM study; Multiferroics; Nano particles; Nano rod; Optical study; XRD analysis;
Conference_Titel :
Nanoscience, Engineering and Technology (ICONSET), 2011 International Conference on
Conference_Location :
Chennai
Print_ISBN :
978-1-4673-0071-1
DOI :
10.1109/ICONSET.2011.6167928