Title :
Fabrication of TiO2 nanofibers by electrospinning technique
Author :
Mathews, Tom ; Antony, Rajini P. ; Ajikumar, P.K. ; Robert, B.
Author_Institution :
Surface & Nanosci. Div., Centre for Atomic Res., Kalpakkam, India
Abstract :
TiO2 nanofibers were synthesized by incorporating sol-gel and electrospinning techniques using polyvinyl pyrrolidone and titanium tetraisopropoxide sol-gel as precursor. The as prepared composite fibres were of ~300 nm average diameter. Calcination of these composite fibres at 500° C in air resulted in pure anatase titania nanofibres, of 84 nm mean diameter with smooth surfaces, without contamination of the other phases. In contrast, surfaces that are more granular evolved when they were calcined at higher temperatures. The phase of the as prepared as well as annealed samples was revealed by micro Raman investigations.This electronic document is a "live" template. The various components of your paper [title, text, heads, etc.] are already defined on the style sheet, as illustrated by the portions given in this document.
Keywords :
Raman spectra; annealing; calcination; electrospinning; fibre reinforced plastics; filled polymers; nanocomposites; nanofabrication; nanofibres; semiconductor growth; semiconductor materials; sol-gel processing; surface roughness; titanium compounds; TiO2; anatase titania nanofibers; annealing; calcination; composite fibres; contamination; electrospinning; microRaman spectra; polyvinyl pyrrolidone; smooth surface; sol-gel method; temperature 500 degC; titanium tetraisopropoxide; Annealing; Spectroscopy; Spinning; Stimulated emission; TiO2 nanofibers; electro spinning;
Conference_Titel :
Nanoscience, Engineering and Technology (ICONSET), 2011 International Conference on
Conference_Location :
Chennai
Print_ISBN :
978-1-4673-0071-1
DOI :
10.1109/ICONSET.2011.6168026