• DocumentCode
    445714
  • Title

    Preparation of enantiopure sultams by intramolecular diels-alder reaction of 1,3-cyclohexadiene-containing vinylsulfonamides

  • Author

    Rogachev, Victor O. ; Metz, Peter

  • Author_Institution
    Tomsk Polytech. Univ., Russia
  • Volume
    2
  • fYear
    2004
  • fDate
    26 June-3 July 2004
  • Firstpage
    76
  • Abstract
    Enantiomerically pure δ-sultams have been prepared by intramolecular [4+2] cycloaddition of N-1-phenylethy substituted vinylsulfonamides with purely thermal activation and under high pressure. An optimized procedure for reductive debenzylation of the resultant δ-sultams is also reported.
  • Keywords
    materials preparation; organic compounds; reduction (chemical); 1,3-cyclohexadiene-containing vinylsulfonamides; N-1-phenylethy substituted vinylsulfonamides; enantiomerically pure δ-sultams; enantiopure sultams; intramolecular cycloaddition; intramolecular diels-alder reaction; reductive debenzylation; thermal activation; Biological materials; Ceramics; Chemicals; Corrosion; Electrical resistance measurement; Gas industry; Mechanical variables measurement; Oxidation; Protection; Testing;
  • fLanguage
    English
  • Publisher
    ieee
  • Conference_Titel
    Science and Technology, 2004. KORUS 2004. Proceedings. The 8th Russian-Korean International Symposium on
  • Print_ISBN
    0-7803-8383-4
  • Type

    conf

  • DOI
    10.1109/KORUS.2004.1555545
  • Filename
    1555545