Title :
Study on the realization of zinc point
Author :
Widiatmo, J.V. ; Sakai, M. ; Yamazawa, K. ; Satou, K. ; Tamba, J. ; Arai, M.
Author_Institution :
Thermometry & Humidity Div., Nat. Metrol. Inst. of Japan, Ibaraki, Japan
Abstract :
Two zinc-point cells were fabricated using high grade zinc samples, impurity elements of one of which were analyzed extensively. Temperature measurements during the solid-liquid coexistence, under which the zinc fixed-point is defined, were conducted, the result of which was used to perform a thermal analysis. Comparisons of zinc-point temperature realized within the newly fabricated cells were also conducted. Zinc-point depression due to impurity elements was calculated based on the chemical element analysis. Evaluation was made on the thermal analysis, the cell comparison results and the chemical element analysis, to lead to an estimation of uncertainty caused by the impurity elements. The present paper outlines the cell fabrication, the temperature measurements and the evaluation of impurity effect to the zinc-point realization.
Keywords :
chemical analysis; furnaces; thermal analysis; zinc; chemical element analysis; high grade zinc samples; impurity elements; solid-liquid coexistence; temperature measurements; thermal analysis; zinc fixed-point; zinc-point cells; zinc-point depression; zinc-point temperature; Chemical analysis; Chemical elements; Fabrication; Impurities; Lead; Performance analysis; Performance evaluation; Temperature measurement; Thermal conductivity; Zinc; cell comparison; fixed point; fixed-point cell; freezing curve; freezing point;
Conference_Titel :
ICCAS-SICE, 2009
Conference_Location :
Fukuoka
Print_ISBN :
978-4-907764-34-0
Electronic_ISBN :
978-4-907764-33-3