Title :
Methyl Trichlorosilane Preparation of Methyl Aluminum Silicate
Author :
Guangxia, Zhang ; Qiaoyun, Zhang ; Zemin, Chen
Author_Institution :
Chem. & Mater. Sci. Inst., Langfang Teachers Coll., Langfang, China
fDate :
July 31 2012-Aug. 2 2012
Abstract :
Methyl trichlorosilane which a waste in the production of silicone prepared methyl aluminum silicate. Methyl trichlorosilane hydrolysate were methyl trihydroxy silane and hydrogen chloride that may be recyclable. Methyl trihydroxy silane and acidified aluminum prepared superfine methyl aluminum silicate. Put methyl trihydroxy silane, sodium hydroxide and acidified aluminum (the mass proportion was 4:2:3) in mixture solvent (the volume ratio of ethanol and water was 3:1), the reaction temperature was 80°C, pH was 10-11, reaction time was 2h, aging time was 4h, 120°C vacuum drying. Manufactrue was characterised by XRD, IR, SEM, and differential thermal analysis.
Keywords :
X-ray diffraction; ageing; differential thermal analysis; drying; infrared spectra; mixtures; scanning electron microscopy; silicones; IR spectra; SEM; XRD; acidified aluminum; aging time; differential thermal analysis; hydrogen chloride; infrared spectrum; methyl trichlorosilane preparation; methyl trihydroxy silane; mixture solvent; pH; silicone prepared methyl aluminum silicate; sodium hydroxide; superfine methyl aluminum silicate; temperature 120 degC; temperature 80 degC; time 2 h; time 4 h; vacuum drying; Aging; Aluminum; Ethanol; Hydrogen; Production; Scanning electron microscopy; Vibrations; Methyl Aluminum Silicate; Methyl Trichlorosilane; Organosilicon;
Conference_Titel :
Digital Manufacturing and Automation (ICDMA), 2012 Third International Conference on
Conference_Location :
GuiLin
Print_ISBN :
978-1-4673-2217-1
DOI :
10.1109/ICDMA.2012.124