Title :
Deposition behaviour of Titanium dioxide (TiO2) nanoparticles during electrophoretic deposition (EPD) technique - Effects of pH
Author :
Fitrah Rabani, A.A. ; Noorsuhana, M.Y.
Author_Institution :
Fac. of Chem. Eng., Univ. Teknol. MARA, Shah Alam, Malaysia
Abstract :
The purpose of this study is to understand the electrophoresis of Titanium dioxide (TiO2) nanoparticles during electrophoretic deposition (EPD) technique. This research was focusing on the effect of pH on the deposition behaviour of Titanium dioxide (TiO2) nanoparticles during electrophoretic deposition (EPD) technique. The ceramic substrates were prepared by using commercial ceramic filter. The TiO2 suspension were prepared by using non-aqueous solvent of alcohol and been characterized using Zeta sizer Nano series. The EPD was performed at 5V pulse-DC for 10 minutes. The deposited TiO2 were then been analyzed by using Field Scanning Electron Microscopy (FE-SEM). It was identified that the IEP was at pH 2.36 and cathodic deposition were observed at all pH except for pH 2. This study has achieved its objective where the different behaviour of TiO2 nanoparticles deposit was identified respected to vary pH. Future works will directed to increased the stability of TiO2 suspension by using poly(acrylic acid) (PAA) for the same goal.
Keywords :
electrophoresis; field emission electron microscopy; nanofabrication; nanoparticles; pH; scanning electron microscopy; solvent effects; suspensions; titanium compounds; DC pulse; EPD technique; FESEM; PAA; TiO2; Zetasizer nano series; alcohol; cathodic deposition; ceramic substrates; commercial ceramic filter; electrophoretic deposition; field scanning electron microscopy; nonaqueous solvent; pH 2.36; poly(acrylic acid); suspension; time 10 min; titanium dioxide nanoparticles; voltage 5 V; Analytical models; Ceramics; Electrodes; Europe; Suspensions; deposition behaviour; electrophoresis; electrophoretic deposition (EPD); titanium dioxide (TiO2) nanoparticles;
Conference_Titel :
Business Engineering and Industrial Applications Colloquium (BEIAC), 2013 IEEE
Conference_Location :
Langkawi
Print_ISBN :
978-1-4673-5967-2
DOI :
10.1109/BEIAC.2013.6560190