Title :
Characteristics of MOD Bi-2212 Thin Films on r-Cut Sapphire With
Buffer Layer
Author :
Shimakage, Hisashi ; Suzuki, Satoshi ; Kawakami, Akira ; Saito, Akihiro ; Takeda, Masanori
Author_Institution :
Grad. Sch. of Sci. & Eng., Ibaraki Univ., Hitachi, Japan
Abstract :
We have studied Bi2Sr2CaCu2O8+δ (Bi-2212) thin films fabrication by a metal organic decomposition method. When the Bi-2212 thin films were prepared on c-cut sapphire substrates, the maximum critical temperature (TC) was 25 K by 820°C air annealing in an electric furnace for 30 min. When the Bi-2212 thin films were prepared on r-cut sapphire substrates with CeO2 buffer layer, the Bi-2212 thin films were grown epitaxially on the CeO2 buffer layer. The maximum TC obtained in the Bi-2212/CeO2/r-cut sapphire was 62.5 K by 840°C air annealing in an electric furnace for 30 min. To improve the surface morphology, face-to-face annealing process was introduced for the Bi-2212/CeO2/r-cut sapphire. By face-to-face annealing, TC was increased up to 65 K, and the critical current density of 1.03 × 105 A/cm2 was obtained at 5 K.
Keywords :
MOCVD; annealing; bismuth compounds; buffer layers; calcium compounds; cerium compounds; critical current density (superconductivity); high-temperature superconductors; sapphire; strontium compounds; superconducting thin films; superconducting transition temperature; surface morphology; vapour phase epitaxial growth; Bi2Sr2CaCu2O-CeO2; MOD Bi-2212 thin films; air annealing; buffer layer; critical current density; epitaxial growth; face-to-face annealing; maximum critical temperature; metalorganic decomposition; r-cut sapphire; surface morphology; temperature 820 C; temperature 840 C; time 30 min; Annealing; Buffer layers; Conductivity; Fabrication; Josephson junctions; Substrates; $hbox{CeO}_{2}$ buffer layer; Bi-2212 thin film; metal-organic decomposition; sapphire;
Journal_Title :
Applied Superconductivity, IEEE Transactions on
DOI :
10.1109/TASC.2013.2248191