Title :
Effect of microwave sintering on structural and magnetic properties of SrFe12O19 nanopowders
Author :
Katlakunta, Sadhana ; Meena, S.S. ; Shinde, R.S. ; Murthy, S.R.
Author_Institution :
Dept. of Phys., Osmania Univ., Hyderabad, India
Abstract :
Nanocrystalline SrFe12O19 has been prepared by microwave hydrothermal method at 473 K/90 min, subsequently annealed at different temperatures using microwaves (2.45GHz). The average particle size of the powders was found to be 48 nm. The plate shape grains were observed in FE-SEM at 1073 K. The crystals exhibited the typical hexagonal ferrite growth habit with a plate-like geometry. The effects of microwave sintering temperature on crystallinity, morphology and magnetic properties have been investigated. The grain sizes of sintered hexaferrites are in the range of 250 to 890 nm. The value of Ms = 58 kA/m and Hc = 125 kA/m was obtained at 1173 K/1h.
Keywords :
annealing; ferrites; field emission electron microscopy; grain size; magnetic particles; magnetisation; nanofabrication; nanomagnetics; nanoparticles; particle size; scanning electron microscopy; sintering; strontium compounds; FESEM; SrFe12O19; annealing; grain sizes; hexaferrites; hexagonal ferrite growth; magnetic properties; magnetization curves; microwave hydrothermal method; microwave sintering; morphological properties; nanocrystalline materials; nanopowders; particle size; plate-like geometry; structural properties; temperature 1073 K; temperature 473 K; time 90 min; Magnetic analysis; Magnetic domains; Random access memory; Silicon; Strontium; Systematics; X-ray scattering; FE-SEM; Microwave-hydrothermal method; TG/DTA; XRD; magnetic properties;
Conference_Titel :
Advanced Nanomaterials and Emerging Engineering Technologies (ICANMEET), 2013 International Conference on
Conference_Location :
Chennai
Print_ISBN :
978-1-4799-1377-0
DOI :
10.1109/ICANMEET.2013.6609368
