• DocumentCode
    842649
  • Title

    Fabrication of fine and homogeneous MgB2 nano powders by spray pyrolysis

  • Author

    Ko, Jae-Woong ; Yoo, Jaimoo ; Kim, Young-Kuk ; Chung, Kook-Chae ; Chung, Hyungsik ; Yoo, Sang-Im

  • Author_Institution
    Sch. of Mater. Sci. & Eng., Seoul Nat. Univ., South Korea
  • Volume
    15
  • Issue
    2
  • fYear
    2005
  • fDate
    6/1/2005 12:00:00 AM
  • Firstpage
    3349
  • Lastpage
    3351
  • Abstract
    Homogeneous nano-sized spherical MgB2 powders were fabricated by spray pyrolysis. The influence of solution concentration, furnace reaction temperature and mass flow of carrier gas on morphology and average particle size were investigated. MgB2 powders were synthesized with or without further heat treatment. For adequate preparation conditions, it has mostly spherical, solid and narrow particle size distribution. Average particle size (X50) distribution was below 100 nm. The critical temperature for the synthesized MgB2 was around 36 K.
  • Keywords
    annealing; flux pinning; grain boundaries; magnesium compounds; nanoparticles; particle size; powders; pyrolysis; superconducting transition temperature; type II superconductors; MgB2; average particle size; carrier gas; flux pinning; furnace reaction temperature; homogeneous MgB2 nano powders; mass flow; morphology; particle size distribution; solution concentration; spray pyrolysis; Critical current density; Fabrication; Grain boundaries; Heat treatment; High temperature superconductors; Materials science and technology; Powders; Spraying; Superconducting materials; Superconductivity; Flux pinning; spray pyrolysis;
  • fLanguage
    English
  • Journal_Title
    Applied Superconductivity, IEEE Transactions on
  • Publisher
    ieee
  • ISSN
    1051-8223
  • Type

    jour

  • DOI
    10.1109/TASC.2005.848889
  • Filename
    1440389