DocumentCode
938630
Title
Improved thermal, structural and electrical properties of epoxy for use at high voltages
Author
Lee, K.Y. ; Lee, K.W. ; Choi, Y.S. ; Par, D.H. ; Lim, K.J.
Author_Institution
Sch. of Electr., Electron. & Inf. Eng., Wonkwang Univ., Iksan, South Korea
Volume
12
Issue
3
fYear
2005
fDate
6/1/2005 12:00:00 AM
Firstpage
566
Lastpage
572
Abstract
In this paper, the epoxy elasticity factors were investigated by thermomechanical analysis (TMA), dynamic mechanical thermal analysis (DMTA), thermogravimetric analysis (TGA) and field emission scanning electron microscope (FESEM) to improve toughness and reduce brittleness of existing epoxy resin. Dumbbell shaped specimens were made and tested at rates of 0, 20 and 35 parts per hundred resins (phr). TMA and DMTA temperatures ranged from -20 to 200 °C and TGA ranged from 0 to 600 °C. The glass transition temperature (Tg) of elastic epoxy was measured by thermal analysis. Also investigated were the thermal expansion coefficient (α), the high-temperature characteristics, modulus and the loss factor (Tan δ). We analyzed the structure using FESEM and have found elastomer particles (elastic-factors) in the elastic epoxy matrix. We have made elastic epoxy by adding elastomer particles to existing epoxy. Generally, the toughness of elastic epoxy can be improved by changing the structure of existing epoxy of poor impact-strength. In addition, we measured the permittivity and Tan δ for investigation of the electrical properties of elastic epoxy. The permittivity and Tan δ depend on the elastomer composition. Namely, the permittivity and Tan δ increase according to the elastomer contents. For experimental analysis results, 20 phr was considered an excellent specimen.
Keywords
dielectric loss measurement; elastomers; epoxy insulators; field emission electron microscopes; glass transition; organic insulating materials; permittivity measurement; thermal analysis; thermal expansion; 0 to 600 degC; Dumbbell shaped specimen; TGA; Tan δ measurement; dynamic mechanical thermal analysis; elastic epoxy; elastic epoxy matrix; elastomer particles; epoxy resin; field emission scanning electron microscope; glass transition temperature; permittivity measurement; thermal expansion coefficient; thermogravimetric analysis; thermomechanical analysis; Elasticity; Electron emission; Epoxy resins; Permittivity; Scanning electron microscopy; Temperature distribution; Testing; Thermal factors; Thermomechanical processes; Voltage;
fLanguage
English
Journal_Title
Dielectrics and Electrical Insulation, IEEE Transactions on
Publisher
ieee
ISSN
1070-9878
Type
jour
DOI
10.1109/TDEI.2005.1453461
Filename
1453461
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